重氮化过程的危险性分析--章仁根的blog

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重氮化过程的危险性分析 | 2010-12-15 8:26:00

重氮化是使芳伯胺变为重氮盐的反应。通常是把含芳胺的有机化合物在酸性介质中与亚硝酸钠作用，使其中的胺基(－NH2)转变为重氮基(－N＝N－)的化学反应。如二硝基重氮酚的制取等。
　　重氮化的火灾危险性分析：
　　(1)重氮化反应的主要火灾危险性在于所产生的重氮盐，如重氮盐酸盐(C6H5N2Cl)、重氮硫酸盐(C6H5N2H504)，特别是含有硝基的重氮盐，如重氮二硝基苯酚[(NO2)2N2C6H2OH]等，它们在温度稍高或光的作用下，即易分解，有的甚至在室温时亦能分解。一般每升高 10℃，分解速度加快两倍。在干燥状态下，有些重氮盐不稳定，活力大，受热或摩擦、撞击能分解爆炸。含重氮盐的溶液若洒落在地上、蒸汽管道上，干燥后亦能引起着火或爆炸。在酸性介质中，有些金属如铁、铜、锌等能促使重氮化合物激烈地分解，甚至引起爆炸。
　　(2)作为重氮剂的芳胺化合物都是可燃有机物质，在一定条件下也有着火和爆炸的危险。
　　(3)重氮化生产过程所使用的亚硝酸钠是无机氧化剂，于175℃时分解能与有机物反应发生着火或爆炸。亚硝酸钠并非氧化剂，所以当遇到比其氧化性强的氧化剂时，又具有还原性，故遇到氯酸钾、高锰酸钾、硝酸铵等强氧化剂时，有发生着火或爆炸的可能。
　　(4)在重氮化的生产过程中，若反应温度过高、亚硝酸钠的投料过快或过量，均会增加亚硝酸的浓度，加速物料的分解，产生大量的氧化氮气体，有引起着火爆炸的危险。

By:章仁根 | 阅读全文 | 回复(28) | 引用通告 | 编辑

标签：重氮化火灾危险性分析

Re:重氮化过程的危险性分析 | 2010-12-15 8:29:26

分析危险性，落实防范措施，确保生产安全。

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原创 | 2016-9-6 17:56:03

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原创 | 2016-9-28 17:29:53

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原创 | 2016-9-30 12:06:15

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Re:在漫画中识别身边的违章 | 2016-10-8 19:34:51

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Re:在漫画中识别身边的违章 | 2016-10-12 21:29:50

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Re:在漫画中识别身边的违章 | 2016-10-12 21:30:22

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Re:在漫画中识别身边的违章 | 2016-10-14 14:30:28

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Re:在漫画中识别身边的违章 | 2016-10-17 18:27:16

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Re:在漫画中识别身边的违章 | 2016-10-19 12:39:47

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Re:在漫画中识别身边的违章 | 2016-10-20 12:23:24

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Re:在漫画中识别身边的违章 | 2016-10-20 23:05:13

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Re:在漫画中识别身边的违章 | 2016-10-22 2:47:00

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Re:在漫画中识别身边的违章 | 2016-10-22 3:23:25

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Re:在漫画中识别身边的违章 | 2016-10-22 16:19:02

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Re:在漫画中识别身边的违章 | 2016-10-23 1:09:47

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Re:在漫画中识别身边的违章 | 2016-10-23 14:31:05

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Re:在漫画中识别身边的违章 | 2017-2-17 23:27:02

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By:kafgk(游客) | 个人主页 | 引用 | 返回 | 删除 | 回复

Re:在漫画中识别身边的违章 | 2017-2-18 14:02:54

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Re:在漫画中识别身边的违章 | 2017-2-18 17:26:22

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Re:在漫画中识别身边的违章 | 2017-2-19 23:10:39

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Re:在漫画中识别身边的违章 | 2017-3-4 15:10:53

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